6J6W
Mutant K23N of heat shock factor 4-DBD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2018-06-16 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 44.632, 65.047, 80.556 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.169 - 1.693 |
R-factor | 0.1727 |
Rwork | 0.171 |
R-free | 0.20520 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.207 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.170 | 1.730 |
High resolution limit [Å] | 1.690 | 1.690 |
Number of reflections | 26197 | |
<I/σ(I)> | 24.1 | |
Completeness [%] | 99.4 | |
Redundancy | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 295 | sodium nitrate |