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6J5R

OspA mutant, PSAM-VLGDV1-form8, grafted short chameleon sequence from alpha-B crystallin

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-17A
Synchrotron sitePhoton Factory
BeamlineBL-17A
Temperature [K]100
Detector technologyPIXEL
Collection date2017-02-20
DetectorDECTRIS PILATUS3 S 6M
Wavelength(s)1.000
Spacegroup nameP 1 21 1
Unit cell lengths33.280, 53.145, 64.651
Unit cell angles90.00, 100.47, 90.00
Refinement procedure
Resolution19.685 - 1.850
R-factor0.2214
Rwork0.220
R-free0.25380
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)6j47
RMSD bond length0.007
RMSD bond angle0.902
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Refinement softwarePHENIX ((1.14_3260: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0001.880
High resolution limit [Å]1.8501.850
Rmerge0.0630.330
Number of reflections18781863
<I/σ(I)>20.72.46
Completeness [%]98.896.2
Redundancy3.12.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8.52770.1 M Tri-HCl pH 8.5, 38% PEG 400

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