6J3X
The Structure of Maltooligosaccharide-forming Amylase from Pseudomonas saccharophila STB07 with Maltotriose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-11-09 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.978910 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.320, 64.650, 169.010 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.470 - 1.620 |
R-factor | 0.1649 |
Rwork | 0.164 |
R-free | 0.18610 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6iwk |
RMSD bond length | 0.010 |
RMSD bond angle | 1.130 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.470 | 4.670 |
High resolution limit [Å] | 1.620 | 1.620 |
Number of reflections | 65292 | |
<I/σ(I)> | 1.38 | |
Completeness [%] | 99.6 | |
Redundancy | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 0.1 M ammonium sulfate, 0.02 M Tris-NCl |