6J3N
RORgammat LBD complexed with Ursonic Acid and SRC2.2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2018-09-27 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.979176 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 61.930, 61.930, 155.870 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.486 - 1.990 |
R-factor | 0.2008 |
Rwork | 0.199 |
R-free | 0.23330 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | CrysalisPro |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.486 | 2.040 |
High resolution limit [Å] | 1.990 | 1.990 |
Number of reflections | 21683 | |
<I/σ(I)> | 19.6 | |
Completeness [%] | 99.9 | |
Redundancy | 24.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 20% PEG3350 0.2M CaCl2 |