6J2A

The structure of HLA-A*3003/NP44

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	DIFFRACTOMETER
Collection date	2018-01-10
Detector	SDMS
Wavelength(s)	0.97853
Spacegroup name	C 1 2 1
Unit cell lengths	155.736, 79.416, 44.744
Unit cell angles	90.00, 93.74, 90.00

Refinement procedure

Resolution	44.649 - 1.400
R-factor	0.1823
Rwork	0.182
R-free	0.19540
RMSD bond length	0.007
RMSD bond angle	0.861
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	CNS
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.450
High resolution limit [Å]	1.400	1.400
Number of reflections	106161
<I/σ(I)>	0.4
Completeness [%]	99.3
Redundancy	6.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	5.6	291	0.1M Tri-Sodium Citrate dihydrate (pH 5.6), 1.0M Lithium Sulfate monohydrate