6J1W

The structure of HLA-A*3001/RT313

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2018-02-11
Detector	SDMS
Wavelength(s)	0.97774
Spacegroup name	P 21 21 2
Unit cell lengths	79.268, 72.025, 78.011
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	44.012 - 1.501
R-factor	0.1891
Rwork	0.188
R-free	0.20550
RMSD bond length	0.013
RMSD bond angle	1.208
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	CNS
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.550
High resolution limit [Å]	1.500	1.500
Number of reflections	71391
<I/σ(I)>	50
Completeness [%]	99.1
Redundancy	12.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	5.5	291	0.1 M sodium citrate tribasic dehydrate (pH 5.5)