6IZH
Crystal structure of deaminase AmnE from Pseudomonas sp. AP-3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 217 |
Detector technology | CCD |
Collection date | 2018-10-05 |
Detector | RIGAKU |
Wavelength(s) | 0.9778 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 170.871, 54.781, 134.594 |
Unit cell angles | 90.00, 101.89, 90.00 |
Refinement procedure
Resolution | 49.511 - 1.754 |
R-factor | 0.1588 |
Rwork | 0.157 |
R-free | 0.19490 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2dyy |
RMSD bond length | 0.007 |
RMSD bond angle | 0.980 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.511 | 1.810 |
High resolution limit [Å] | 1.754 | 1.760 |
Rmerge | 0.901 | 0.535 |
Rpim | 0.044 | 0.244 |
Number of reflections | 120742 | 19456 |
<I/σ(I)> | 28.25 | |
Completeness [%] | 99.3 | |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9.6 | 293.15 | CAPSO,Magnesium chloridehexahydrate,PEG4000. |