6IXW
pCBH ParM non-polymerisable quadruple mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE TPS 05A |
Synchrotron site | NSRRC |
Beamline | TPS 05A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-10-12 |
Detector | RAYONIX MX300-HS |
Wavelength(s) | 1 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 164.153, 93.922, 114.699 |
Unit cell angles | 90.00, 131.55, 90.00 |
Refinement procedure
Resolution | 19.974 - 3.253 |
R-factor | 0.1607 |
Rwork | 0.158 |
R-free | 0.21400 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 20.000 | 20.000 | 3.310 |
High resolution limit [Å] | 3.250 | 8.590 | 3.250 |
Rmerge | 0.143 | 0.040 | 0.574 |
Rmeas | 0.170 | 0.048 | 0.696 |
Rpim | 0.091 | 0.026 | 0.388 |
Number of reflections | 20481 | 1056 | 995 |
<I/σ(I)> | 6.8 | ||
Completeness [%] | 99.9 | 100 | 99.1 |
Redundancy | 3.5 | 3.4 | 3.2 |
CC(1/2) | 0.995 | 0.562 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 288 | 28% PEG 400 0.1 M Hepes 0.15 M MgCl2 pH 7.5 |