6IX3
The structure of LepI complex with SAM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-23 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97930 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 161.301, 61.792, 113.318 |
Unit cell angles | 90.00, 113.55, 90.00 |
Refinement procedure
Resolution | 36.959 - 2.130 |
R-factor | 0.1774 |
Rwork | 0.176 |
R-free | 0.21140 |
Structure solution method | SAD |
RMSD bond length | 0.004 |
RMSD bond angle | 0.775 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX (v1.12_2829) |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.180 |
High resolution limit [Å] | 2.130 | 2.130 |
Rmerge | 0.192 | 2.028 |
Number of reflections | 56044 | 2744 |
<I/σ(I)> | 19.553 | |
Completeness [%] | 97.9 | |
Redundancy | 9.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.2M sodium chloride, 0.1M MES(pH 6.0), 20%(w/v) PEG 6000 |