6IW1
Crystal structure of YFV-17D sE in postfusion state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-09-20 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97853 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 140.558, 88.275, 128.953 |
Unit cell angles | 90.00, 107.06, 90.00 |
Refinement procedure
Resolution | 39.955 - 3.100 |
R-factor | 0.217 |
Rwork | 0.215 |
R-free | 0.25390 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.151 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 39.900 |
High resolution limit [Å] | 3.100 | 3.100 |
Number of reflections | 26089 | |
<I/σ(I)> | 7.8 | |
Completeness [%] | 99.4 | |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 291 | 0.1 M HEPES pH 7.0, 30% v/v Jeffamine, M-600, pH 7.0 |