6IVC

The full length of TGEV nsp1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	CCD
Collection date	2017-07-10
Detector	ADSC QUANTUM 315
Wavelength(s)	1.0
Spacegroup name	P 1 21 1
Unit cell lengths	36.164, 67.008, 90.101
Unit cell angles	90.00, 93.98, 90.00

Refinement procedure

Resolution	34.315 - 1.800
R-factor	0.1836
Rwork	0.181
R-free	0.23210
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3zbd
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHENIX
Refinement software	PHENIX (1.14_3260)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	34.315	1.845
High resolution limit [Å]	1.800	1.800
Rmerge	0.056	0.476
Number of reflections	38588	38588
<I/σ(I)>	20.16
Completeness [%]	96.9
Redundancy	4.18

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	PEG3350, Lithium chloride