6IS9
Crystal Structure of ZmMOC1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-01-13 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.978 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.373, 74.604, 97.381 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.868 - 1.860 |
R-factor | 0.1762 |
Rwork | 0.174 |
R-free | 0.20940 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.940 |
High resolution limit [Å] | 1.800 | 3.880 | 1.860 |
Rmerge | 0.123 | 0.052 | 0.963 |
Rmeas | 0.131 | 0.056 | 1.024 |
Rpim | 0.044 | 0.019 | 0.343 |
Number of reflections | 31645 | 3368 | 3101 |
<I/σ(I)> | 6.5 | ||
Completeness [%] | 99.5 | 99.1 | 99.5 |
Redundancy | 8.5 | 8.1 | 8.6 |
CC(1/2) | 0.998 | 0.837 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 7.6 | 298 | 0.07 M Bis-tris propane pH 7.6, 20% PEG 3350, 0.03 M citrate acid |