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6IRX

Crystal structure of the zebrafish cap-specific adenosine methyltransferase

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06DA
Synchrotron siteSLS
BeamlineX06DA
Temperature [K]100
Detector technologyPIXEL
Collection date2017-09-04
DetectorDECTRIS EIGER X 16M
Wavelength(s)0.979
Spacegroup nameP 21 21 21
Unit cell lengths71.545, 84.132, 93.084
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution47.033 - 2.000
R-factor0.1923
Rwork0.191
R-free0.21540
Structure solution methodSAD
Data reduction softwareXDS
Data scaling softwareAimless (0.7.2)
Phasing softwareSHELXD
Refinement softwarePHENIX (1.13_2998)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]47.03347.0302.050
High resolution limit [Å]2.0008.9402.000
Rmerge0.1350.0851.054
Rmeas0.1410.0891.098
Rpim0.0400.0260.303
Number of reflections386945112822
<I/σ(I)>10.1
Completeness [%]100.099.6100
Redundancy12.41112.9
CC(1/2)0.9960.9900.913
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.529311% PEG 3350, 0.1M potassium thiocyanate, 0.1M bis-Tris propane

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