6IRC
C-terminal domain of Drosophila phospholipase b NORPA, methylated
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-05-16 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9793 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 119.209, 119.209, 116.059 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.957 - 3.538 |
R-factor | 0.2467 |
Rwork | 0.244 |
R-free | 0.29550 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.560 |
High resolution limit [Å] | 3.500 | 9.480 | 3.500 |
Rmerge | 0.127 | 0.051 | 0.612 |
Rmeas | 0.133 | 0.054 | 0.648 |
Rpim | 0.040 | 0.017 | 0.203 |
Total number of observations | 68157 | ||
Number of reflections | 5961 | 331 | 300 |
<I/σ(I)> | 8.2 | ||
Completeness [%] | 94.4 | 87.1 | 94.9 |
Redundancy | 11.4 | 9.2 | 11.4 |
CC(1/2) | 0.998 | 0.702 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIQUID DIFFUSION | 289 | 3.8M Sodium Formate, 100mM Bis-tris Propane |