6IR8
Rice WRKY/DNA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-19 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9778 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 48.225, 87.831, 99.691 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.916 - 2.300 |
R-factor | 0.1955 |
Rwork | 0.193 |
R-free | 0.24440 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1aut |
RMSD bond length | 0.008 |
RMSD bond angle | 0.944 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.850 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.151 | 0.531 |
Rpim | 0.024 | 0.105 |
Number of reflections | 9748 | |
<I/σ(I)> | 24.4 | |
Completeness [%] | 100.0 | |
Redundancy | 12.1 | |
CC(1/2) | 0.997 | 0.972 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 278 | 0.27 M calcium acetate hydrate, 21% (w/v) PEG 3350 |