6IQU
Crystal structure of Prc with PDZ domain deletion in complex with NlpI
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE TPS 05A |
Synchrotron site | NSRRC |
Beamline | TPS 05A |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2018-09-19 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 0.99984 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 105.827, 151.082, 148.380 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.800 - 2.900 |
R-factor | 0.19398 |
Rwork | 0.192 |
R-free | 0.23340 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5wql |
RMSD bond length | 0.010 |
RMSD bond angle | 1.765 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 (V712) |
Phasing software | PHASER (2.70) |
Refinement software | REFMAC (5.8.0232) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.000 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.057 | 0.201 |
Rmeas | 0.088 | 0.276 |
Rpim | 0.042 | 0.141 |
Number of reflections | 25531 | 1987 |
<I/σ(I)> | 18.95 | 4.39 |
Completeness [%] | 95.9 | 76 |
Redundancy | 4.4 | 3.4 |
CC(1/2) | 0.963 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | PEG3350, sodium citrate tribasic dihydrate |