6IO9
The structure of apo-UdgX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-05 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 36.572, 50.958, 54.367 |
Unit cell angles | 90.00, 104.56, 90.00 |
Refinement procedure
Resolution | 36.606 - 1.900 |
R-factor | 0.1917 |
Rwork | 0.190 |
R-free | 0.22520 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ui0 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.633 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.093 | 0.340 |
Number of reflections | 15400 | 1486 |
<I/σ(I)> | 22.6 | 4.7 |
Completeness [%] | 97.2 | 97.1 |
Redundancy | 3.4 | 3.5 |
CC(1/2) | 0.980 | 0.840 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5.6 | 298 | 0.05M MES 5.6, 2.45M (NH4)2SO4 and 0.1M MgCl2 |