6IM5
YAP-binding domain of human TEAD1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 93 |
Detector technology | CCD |
Collection date | 2018-07-26 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.9794 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 36.537, 89.356, 135.569 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.412 - 1.701 |
R-factor | 0.1967 |
Rwork | 0.195 |
R-free | 0.23020 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3kys |
RMSD bond length | 0.006 |
RMSD bond angle | 0.899 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.730 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.066 | 0.290 |
Number of reflections | 49632 | 2451 |
<I/σ(I)> | 35.4 | |
Completeness [%] | 99.5 | |
Redundancy | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 4% (v/v) 2-propanol, 100 mM sodium phosphate dibasic/citric acid (pH 4.5), and 200 mM lithium sulfate |