6ILF
CRYSTAL STRUCTURE OF BAT MHC CLASS I PTAL-N*01:01 FOR 2.7 ANGSTROM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2018-04-13 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 0.97892 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 72.126, 87.871, 133.992 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.713 - 2.700 |
R-factor | 0.219 |
Rwork | 0.215 |
R-free | 0.29250 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3vfn |
RMSD bond length | 0.003 |
RMSD bond angle | 0.646 |
Data reduction software | HKL-3000 |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.000 |
High resolution limit [Å] | 1.970 | 1.970 |
Rmerge | 0.213 | 0.614 |
Number of reflections | 12065 | 1349 |
<I/σ(I)> | 2.6 | |
Completeness [%] | 75.5 | |
Redundancy | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.2M Lithium sulfate monohydrate, 0.1M BIS-TRIS pH 6.5, 25%(w/v) Polyethylene glycol 3,350 |