6IGE
Crystal structure of Human Papillomavirus type 33 pentamer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2013-10-20 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9795 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 98.827, 171.937, 145.692 |
Unit cell angles | 90.00, 97.04, 90.00 |
Refinement procedure
Resolution | 48.198 - 2.900 |
R-factor | 0.2111 |
Rwork | 0.210 |
R-free | 0.24030 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5y9e |
RMSD bond length | 0.003 |
RMSD bond angle | 0.648 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.970 |
High resolution limit [Å] | 2.900 | 2.920 |
Number of reflections | 105277 | 5220 |
<I/σ(I)> | 14.2 | |
Completeness [%] | 99.8 | |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 0.2 M magnesium formate, 13.5% (w/v) PEG 3350 |