6IFW
crystal structure of chimeric construct of KsgA with loop 1 from erm
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 60.220, 81.000, 120.860 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.400 - 2.950 |
R-factor | 0.20622 |
Rwork | 0.201 |
R-free | 0.29418 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.588 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | Auto-Rickshaw |
Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.026 |
High resolution limit [Å] | 2.950 | 2.950 |
Number of reflections | 15977 | |
<I/σ(I)> | 27.76 | 4.25 |
Completeness [%] | 99.6 | 100 |
Redundancy | 10.2 | 10 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 4% Tacsimate, 15% PEG 3350 |