6IF4
Crystal structure of Tbtudor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-01-22 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9789 |
Spacegroup name | P 1 |
Unit cell lengths | 29.389, 34.274, 37.470 |
Unit cell angles | 113.58, 100.53, 102.90 |
Refinement procedure
Resolution | 32.710 - 1.934 |
R-factor | 0.2084 |
Rwork | 0.206 |
R-free | 0.24880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4pl6 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.710 | 2.040 |
High resolution limit [Å] | 1.930 | 1.930 |
Rmerge | 0.115 | 0.652 |
Rmeas | 0.134 | 0.761 |
Rpim | 0.068 | 0.391 |
Number of reflections | 8625 | 1246 |
<I/σ(I)> | 8.9 | 2.5 |
Completeness [%] | 92.6 | 91.8 |
Redundancy | 3.8 | 3.7 |
CC(1/2) | 0.995 | 0.780 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.1M Bis-Tris, 3M NaCl pH6.5 |