6IE6
Crystal structure of ADCP1 tandem Agenet domain 3-4 in complex with H3K9me2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-10-11 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9792 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 56.891, 56.891, 210.005 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 31.963 - 1.700 |
R-factor | 0.1906 |
Rwork | 0.186 |
R-free | 0.23200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.032 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.730 |
High resolution limit [Å] | 1.700 | 4.610 | 1.700 |
Rmerge | 0.066 | 0.053 | 0.724 |
Rmeas | 0.072 | 0.058 | 0.790 |
Rpim | 0.028 | 0.022 | 0.309 |
Total number of observations | 129592 | ||
Number of reflections | 22285 | 1307 | 1096 |
<I/σ(I)> | 10.7 | ||
Completeness [%] | 95.7 | 94.1 | 97 |
Redundancy | 5.8 | 6.3 | 6.1 |
CC(1/2) | 0.997 | 0.793 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 289 | 0.1M HEPES pH 7.5, 2.0M Ammonium formate |