6IE4
Crystal structure of ADCP1 tandem Agenet domain 1-2 in complex with H3K9me1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-10-11 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9792 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 42.515, 67.529, 116.679 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.147 - 2.696 |
R-factor | 0.2084 |
Rwork | 0.202 |
R-free | 0.26890 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.136 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.14rc3_3206: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.750 |
High resolution limit [Å] | 2.696 | 7.320 | 2.700 |
Rmerge | 0.066 | 0.040 | 0.295 |
Rmeas | 0.081 | 0.049 | 0.363 |
Rpim | 0.046 | 0.028 | 0.209 |
Number of reflections | 9743 | 756 | 808 |
<I/σ(I)> | 9 | ||
Completeness [%] | 89.1 | 85.5 | 91.9 |
Redundancy | 2.5 | 2.7 | 2.5 |
CC(1/2) | 0.996 | 0.895 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 289 | 0.2M Ammonium acetate, 30% PEG 4000, 0.1M Sodium acetate pH 5.0 |