6ICY
Crystal structure of H7 hemagglutinin mutant H7-AGTL ( V186G, P221T) from the influenza virus A/Anhui/1/2013 (H7N9)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-04-27 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97892 |
Spacegroup name | H 3 2 |
Unit cell lengths | 116.544, 116.544, 294.996 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.350 - 2.403 |
R-factor | 0.2448 |
Rwork | 0.244 |
R-free | 0.26650 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.668 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.350 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 30407 | |
<I/σ(I)> | 26.39 | |
Completeness [%] | 99.9 | |
Redundancy | 10.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1M Sodium Chloride, 0.1M HEPES pH7.5, 1.6M Ammonium Sulfate |