6ICI
Crystal structure of human MICAL3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-06-29 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 65.211, 93.466, 71.568 |
Unit cell angles | 90.00, 92.37, 90.00 |
Refinement procedure
Resolution | 47.200 - 2.300 |
R-factor | 0.1735 |
Rwork | 0.172 |
R-free | 0.21440 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4txi |
RMSD bond length | 0.009 |
RMSD bond angle | 0.967 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.200 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 38165 | 5163 |
<I/σ(I)> | 16.89 | 2.72 |
Completeness [%] | 99.7 | 99.8 |
Redundancy | 4.85 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1M Bicine-NaOH pH 9.2, 7% MPD |