6IAJ
Sixty minutes iron loaded Rana Catesbeiana H' ferritin variant H54N
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-10-08 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.95372 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 184.130, 184.130, 184.130 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 23.980 - 1.620 |
R-factor | 0.15525 |
Rwork | 0.154 |
R-free | 0.18368 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4lqh |
RMSD bond length | 0.009 |
RMSD bond angle | 1.549 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.600 | 1.710 |
High resolution limit [Å] | 1.620 | 1.620 |
Rmerge | 0.115 | 0.390 |
Rmeas | 0.130 | 0.463 |
Rpim | 0.045 | 0.180 |
Number of reflections | 34490 | 4928 |
<I/σ(I)> | 10.5 | 3.6 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.8 | 6.4 |
CC(1/2) | 0.995 | 0.898 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9 | 281 | 1.6-2.0 M MgCl2 and 0.1 M bicine pH 9.0 |