6I25
Flavin Analogue Sheds Light on Light-Oxygen-Voltage Domain Mechanism
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-12 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 64 2 2 |
Unit cell lengths | 106.287, 106.287, 67.859 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 54.620 - 1.970 |
R-factor | 0.17901 |
Rwork | 0.177 |
R-free | 0.22230 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5a8b |
RMSD bond length | 0.014 |
RMSD bond angle | 1.697 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.620 | 2.020 |
High resolution limit [Å] | 1.970 | 1.970 |
Number of reflections | 16503 | |
<I/σ(I)> | 7.9 | |
Completeness [%] | 100.0 | |
Redundancy | 20.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1.5-3 M Na malonate, 0.1 M Tris.acetate |