6I0S

Crystal structure of DmTailor in complex with UMPNPP

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-11-03
Detector	DECTRIS PILATUS 2M-F
Wavelength(s)	1.00767
Spacegroup name	P 31 2 1
Unit cell lengths	61.183, 61.183, 167.380
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	44.768 - 1.900
R-factor	0.1897
Rwork	0.188
R-free	0.21880
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	5w0b
RMSD bond length	0.011
RMSD bond angle	0.884
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX ((1.14_3260: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.770	2.010
High resolution limit [Å]	1.900	1.900
Number of reflections	29527
<I/σ(I)>	15.81	1.4
Completeness [%]	100.0	100
Redundancy	19.6	19
CC(1/2)	0.999	0.534

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	293	20 % (v/v) glycerol ethoxylate