6I0Q
Crystal structure of BTB domain of KCTD16 hexamer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-03 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.8 |
Spacegroup name | P 65 |
Unit cell lengths | 62.407, 62.407, 41.861 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 33.095 - 2.300 |
R-factor | 0.1894 |
Rwork | 0.186 |
R-free | 0.23460 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5a15 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.564 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11_2567: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.860 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.200 | 1.372 |
Rmeas | 0.229 | 1.540 |
Rpim | 0.104 | 0.690 |
Number of reflections | 4228 | 403 |
<I/σ(I)> | 8.1 | 1.8 |
Completeness [%] | 100.0 | 100 |
Redundancy | 9.1 | 9.4 |
CC(1/2) | 0.994 | 0.540 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M ammonium sulfate and 20% PEG 3350 |