6HYV
THE GLIC PENTAMERIC LIGAND-GATED ION CHANNEL MUTANT Y119A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 193 |
Detector technology | PIXEL |
Collection date | 2016-12-18 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.9785 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 180.810, 132.380, 159.650 |
Unit cell angles | 90.00, 102.22, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.800 |
R-factor | 0.2093 |
Rwork | 0.209 |
R-free | 0.22120 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.130 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.230 | 2.850 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 90262 | |
<I/σ(I)> | 9.7 | |
Completeness [%] | 99.8 | |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 291 | 12-14.5% PEG4K; 15% GLycerol; 400 mM NaSCN; 3% DMSO; 100mM NaAcetate pH 4 |