6HXB
SERCA2a from pig heart
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 77 |
Detector technology | PIXEL |
Collection date | 2014-09-19 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1 |
Spacegroup name | P 1 2 1 |
Unit cell lengths | 116.995, 51.776, 125.604 |
Unit cell angles | 90.00, 106.13, 90.00 |
Refinement procedure
Resolution | 41.724 - 4.000 |
Rwork | 0.310 |
R-free | 0.35440 |
RMSD bond length | 0.010 |
RMSD bond angle | 0.533 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.700 | 4.500 |
High resolution limit [Å] | 4.000 | 4.000 |
Number of reflections | 12416 | |
<I/σ(I)> | 4.2 | |
Completeness [%] | 98.7 | |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 292.15 | 21% PEG2000 monomethyl ether, 20% glycerol, 100 mM NaCl, 5% tert-BuOH and 2.4% Zwittergent-3-08 |