6HV1
The apo structure of Dps from Listeria innocua before soaking experiments with Zn, Co and La
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALBA BEAMLINE XALOC |
| Synchrotron site | ALBA |
| Beamline | XALOC |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-11-11 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 1 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 84.710, 84.710, 263.610 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 44.761 - 2.547 |
| R-factor | 0.1921 |
| Rwork | 0.190 |
| R-free | 0.22730 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.796 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.761 | 2.610 |
| High resolution limit [Å] | 2.547 | 2.547 |
| Number of reflections | 59885 | |
| <I/σ(I)> | 9.9 | |
| Completeness [%] | 99.9 | |
| Redundancy | 4.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 20% PEG3350, pH 7 |
