6HRJ
Apo - YndL
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SEALED TUBE |
| Source details | OXFORD DIFFRACTION NOVA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2016-11-04 |
| Detector | OXFORD ONYX CCD |
| Wavelength(s) | 1.541 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 38.612, 47.284, 99.893 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 15.750 - 1.700 |
| R-factor | 0.17902 |
| Rwork | 0.177 |
| R-free | 0.21253 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.668 |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0232) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 15.750 | 1.760 |
| High resolution limit [Å] | 1.700 | 1.700 |
| Number of reflections | 20566 | |
| <I/σ(I)> | 22.7 | |
| Completeness [%] | 99.0 | |
| Redundancy | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291 | 1 Ammonium Sulphate, 0.15 M Sodium Citrate |
