6HRI
Native YndL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-07-10 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97622 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 38.670, 46.860, 100.070 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.070 - 1.030 |
R-factor | 0.17414 |
Rwork | 0.173 |
R-free | 0.18942 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.505 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0232) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.200 | 1.070 |
High resolution limit [Å] | 1.030 | 1.030 |
Number of reflections | 76651 | |
<I/σ(I)> | 18.67 | |
Completeness [%] | 85.0 | |
Redundancy | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 1 Ammonium sulphate, 0.15 Sodium citrate |