6HP3
ARBITRIUM PEPTIDE RECEPTOR FROM SPBETA PHAGE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-12-12 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97925 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 78.907, 251.202, 95.077 |
Unit cell angles | 90.00, 90.89, 90.00 |
Refinement procedure
Resolution | 125.600 - 2.700 |
R-factor | 0.22019 |
Rwork | 0.219 |
R-free | 0.24970 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.018 |
RMSD bond angle | 2.168 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 251.200 | 2.850 |
High resolution limit [Å] | 2.700 | 2.700 |
Number of reflections | 101076 | |
<I/σ(I)> | 8.1 | |
Completeness [%] | 100.0 | |
Redundancy | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 294 | PEG 3500, sodium chloride, hepes |