6HO7
TRANSCRIPTIONAL REPRESSOR ETHR FROM MYCOBACTERIUM TUBERCULOSIS IN COMPLEX WITH BDM44814
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-12-06 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.00 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 120.967, 120.967, 33.697 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.550 - 2.500 |
R-factor | 0.1831 |
Rwork | 0.180 |
R-free | 0.23670 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.586 |
Data reduction software | iMOSFLM |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0232) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.700 | 2.640 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.146 | 0.859 |
Number of reflections | 9145 | 1280 |
<I/σ(I)> | 14 | 3.3 |
Completeness [%] | 99.7 | 98.4 |
Redundancy | 10.5 | 10.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.7 | 293 | 1.4-1.6 ammonium sulfate, 15% glycerol, 100 mM MES |