6HK8

Crystal structure of TEX12 delta-Ctip

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-02-18
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9796
Spacegroup name	P 65 2 2
Unit cell lengths	47.970, 47.970, 210.980
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	41.543 - 2.111
R-factor	0.2307
Rwork	0.229
R-free	0.25800
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	Quark decoys
RMSD bond length	0.002
RMSD bond angle	0.316
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	AMPLE
Refinement software	PHENIX ((dev_3126: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	52.750	2.150
High resolution limit [Å]	2.110	2.110
Rmeas	0.082	2.330
Rpim	0.014	0.374
Number of reflections	8428	432
<I/σ(I)>	28.1	2.4
Completeness [%]	92.7	100
Redundancy	34.5	37.5
CC(1/2)	1.000	0.890

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	25% (v/v) 1,4-dioxane, 20% ethylene glycol