6HH4
ADP-ribosylserine hydrolase ARH3 of Latimeria chalumnae in complex with ADP-ribosyl-L-arginine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-08-08 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9686 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 67.145, 96.642, 105.908 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 71.390 - 1.660 |
R-factor | 0.16965 |
Rwork | 0.169 |
R-free | 0.18994 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2foz |
RMSD bond length | 0.012 |
RMSD bond angle | 1.531 |
Data reduction software | XDS |
Data scaling software | DIALS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0222) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 71.390 | 1.700 |
High resolution limit [Å] | 1.660 | 1.660 |
Rmerge | 0.089 | 1.524 |
Rmeas | 0.101 | 1.733 |
Rpim | 0.047 | 0.809 |
Number of reflections | 82067 | 5982 |
<I/σ(I)> | 9.9 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 8.3 | 8.4 |
CC(1/2) | 0.997 | 0.676 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 293.15 | 200 MM AMMONIUM ACETATE, 25 % (W/V), PEG4000, 100 MM CITRATE PH 5.6 |