6HGC

Structure of Calypso in complex with DEUBAD of ASX

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID30B
Synchrotron site	ESRF
Beamline	ID30B
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-09-01
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.9747
Spacegroup name	P 61 2 2
Unit cell lengths	119.505, 119.505, 408.900
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	72.729 - 3.020
R-factor	0.2695
Rwork	0.268
R-free	0.29170
RMSD bond length	0.003
RMSD bond angle	0.565
Refinement software	PHENIX (1.12_2829)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	103.490	3.120
High resolution limit [Å]	3.020	3.020
Number of reflections	31261
<I/σ(I)>	13.3
Completeness [%]	89.3
Redundancy	18.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7	293	6% PEG MME 5K, 0.1 M HEPES pH 7.0, 5 % Tacsimate