6HDS
Crystal Structure of apo short afifavidin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-11-22 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 41.991, 64.952, 68.114 |
Unit cell angles | 90.00, 100.07, 90.00 |
Refinement procedure
Resolution | 46.700 - 1.740 |
R-factor | 0.18679 |
Rwork | 0.184 |
R-free | 0.23066 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ew1 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.559 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0230) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 67.060 | 1.770 |
High resolution limit [Å] | 1.740 | 1.740 |
Number of reflections | 35450 | |
<I/σ(I)> | 11.6 | |
Completeness [%] | 95.7 | |
Redundancy | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 293 | 1.3-1.5M Ammonium Sulfate, 0.1M Acetate pH 5.0 |