6HCL
Crystal structure of a MFS transporter with Ligand at 2.69 Angstroem resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-08 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 103.423, 200.016, 63.323 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.826 - 2.500 |
R-factor | 0.24 |
Rwork | 0.239 |
R-free | 0.25930 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6g9x |
RMSD bond length | 0.007 |
RMSD bond angle | 0.911 |
Data reduction software | XDS (Jan 26, 2018 (BUILT 20180302)) |
Data scaling software | autoPROC (1.0.5 (20170920)) |
Phasing software | PHASER (2.8.1) |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.520 | 2.680 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmeas | 0.118 | 5.100 |
Rpim | 0.020 | 0.900 |
Number of reflections | 30961 | 1341 |
<I/σ(I)> | 40.8 | 1.3 |
Completeness [%] | 94.4 | 88.1 |
Redundancy | 55.9 | 57.2 |
CC(1/2) | 1.000 | 0.590 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 291.15 | zinc bromide, HEPES, jeffamine ED-2003 |