6HBM
Crystal structure of MSMEG_1712 from Mycobacterium smegmatis in complex with alpha-L-arabinofuranose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-02-03 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1 |
Spacegroup name | I 41 2 2 |
Unit cell lengths | 119.500, 119.500, 234.770 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.950 - 2.760 |
R-factor | 0.221 |
Rwork | 0.218 |
R-free | 0.27900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6hb0 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.150 |
Data reduction software | XDS |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 106.500 | 3.190 |
High resolution limit [Å] | 2.750 | 2.750 |
Number of reflections | 63068 | |
<I/σ(I)> | 17.5 | |
Completeness [%] | 92.9 | |
Redundancy | 25.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | 0.1 M Tris, pH 8.0 21 % PEG 400 0.325 M NaOAc 0.1 M NaCl |