6H9O
Complex of the periplasmic domains of bacterial cell division proteins FtsQ and FtsB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-22 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97950 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 117.221, 48.011, 131.619 |
Unit cell angles | 90.00, 112.40, 90.00 |
Refinement procedure
Resolution | 29.834 - 2.800 |
R-factor | 0.2322 |
Rwork | 0.230 |
R-free | 0.27700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vh1 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.637 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.950 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.077 | 0.744 |
Rpim | 0.051 | 0.488 |
Number of reflections | 15922 | 2374 |
<I/σ(I)> | 10.6 | 1.8 |
Completeness [%] | 98.5 | 99.7 |
Redundancy | 3.2 | 3.3 |
CC(1/2) | 0.998 | 0.686 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 | 293 | 0.057 M potassium thiocyanate, 10 % PEG 550 MME, 0.1 M sodium cacodylate pH 6.5. |