Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 273.15 |
| Detector technology | CCD |
| Collection date | 2015-07-10 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.97620 |
| Spacegroup name | P 6 |
| Unit cell lengths | 123.023, 123.023, 60.880 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 40.269 - 2.892 |
| R-factor | 0.2065 |
| Rwork | 0.205 |
| R-free | 0.23730 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2c9o |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.424 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.13_2992: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 52.859 | 2.940 |
| High resolution limit [Å] | 2.892 | 2.892 |
| Rmerge | 0.111 | |
| Rmeas | 0.129 | |
| Rpim | 0.063 | |
| Number of reflections | 11583 | |
| <I/σ(I)> | 11.3 | |
| Completeness [%] | 97.0 | |
| Redundancy | 3.9 | |
| CC(1/2) | 0.996 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6 | 303.15 | PEG 3350, Magnesium Chloride |
