6H74
The molybdenum storage protein - L131H
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-10-08 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.738 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 114.270, 114.270, 234.140 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.480 - 1.801 |
R-factor | 0.1791 |
Rwork | 0.178 |
R-free | 0.19970 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ndo |
RMSD bond length | 0.012 |
RMSD bond angle | 2.480 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.984 | |
Rmeas | 0.048 | 1.217 |
Number of reflections | 154702 | |
<I/σ(I)> | 23 | 1 |
Completeness [%] | 97.6 | 84 |
Redundancy | 5.9 | |
CC(1/2) | 0.999 | 0.763 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 0.1 M sodium citrate, pH 5.6, 1 M ammonium phosphate, 20% glycerol |