6H71
GI.1 human norovirus protruding domain in complex with Nano-94
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-03-19 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.978950 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 94.890, 111.060, 122.460 |
Unit cell angles | 90.00, 99.81, 90.00 |
Refinement procedure
Resolution | 49.400 - 2.313 |
R-factor | 0.1937 |
Rwork | 0.193 |
R-free | 0.21700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zl5 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.620 |
Data reduction software | XDS (VERSION Nov 1, 2016) |
Data scaling software | XSCALE (VERSION Nov 1, 2016) |
Phasing software | PHASER (VERSION Nov 1, 2016) |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.400 | 2.400 |
High resolution limit [Å] | 2.310 | 2.310 |
Rmerge | 0.050 | 0.543 |
Rmeas | 0.061 | 0.656 |
Rpim | 0.034 | 0.362 |
Number of reflections | 53187 | 5051 |
<I/σ(I)> | 14.21 | 2.08 |
Completeness [%] | 97.2 | 92.74 |
Redundancy | 2.9 | 2.9 |
CC(1/2) | 0.999 | 0.874 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.1 M sodium citrate (pH 5.5) and 20% (w/v) PEG3000 |