6H6Z
GI.1 human norovirus protruding domain in complex with Nano-62
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-09-25 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9677 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 172.240, 89.640, 61.920 |
Unit cell angles | 90.00, 107.80, 90.00 |
Refinement procedure
Resolution | 46.672 - 2.085 |
R-factor | 0.1801 |
Rwork | 0.178 |
R-free | 0.21670 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zl5 |
RMSD bond length | 0.008 |
RMSD bond angle | 0.893 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.670 | 2.160 |
High resolution limit [Å] | 2.090 | 2.090 |
Rmerge | 0.071 | 0.554 |
Number of reflections | 51659 | |
<I/σ(I)> | 11.2 | 1.7 |
Completeness [%] | 96.9 | 82.8 |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.1 M sodium citrate (pH 5.5) and 20% (w/v) PEG3000 |