6H4F
TarP-3RboP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-10-05 |
| Detector | DECTRIS PILATUS 2M |
| Wavelength(s) | 1.00000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 95.610, 217.270, 123.990 |
| Unit cell angles | 90.00, 91.38, 90.00 |
Refinement procedure
| Resolution | 49.750 - 2.180 |
| R-factor | 0.17365 |
| Rwork | 0.172 |
| R-free | 0.20478 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6h1j |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.226 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0230) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.800 | 2.220 |
| High resolution limit [Å] | 2.180 | 2.180 |
| Number of reflections | 262098 | |
| <I/σ(I)> | 11.9 | |
| Completeness [%] | 100.0 | |
| Redundancy | 7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.7 | 293 | 25% PEG 3350, 250 mM magnesium chloride, 0.1 M sodium citrate, pH 5.7. |
