6H2N
TarP-UDP-GlcNAc-Mg
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-04-10 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.91841 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 43.850, 95.270, 130.220 |
Unit cell angles | 90.00, 93.49, 90.00 |
Refinement procedure
Resolution | 47.630 - 1.950 |
R-factor | 0.18048 |
Rwork | 0.178 |
R-free | 0.22613 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.211 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHARP |
Refinement software | REFMAC (5.8.0230) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.600 | 2.000 |
High resolution limit [Å] | 1.950 | 1.950 |
Number of reflections | 77771 | |
<I/σ(I)> | 9.2 | |
Completeness [%] | 99.9 | |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.7 | 293 | 25% PEG 3350, 250 mM magnesium chloride, 0.1 M sodium citrate, pH 5.7. |